Spark plasma sintering of CNT-NiAl nanocomposites – Process parameter, densification mechanism, and grain analysis

Full densification of Molybdenum powders using Spark Plasma Sintering

Pure molybdenum powder was sintered using Spark Plasma Sintering under various temperatures, and holding times, under a pressure of 77 MPa and a heating rate at 700°C/min. After sintering, a carbide layer was observed at the surface. The carbide layer thickness, the relative density of the sample as well as the microhardness and the grain size of Mo were measured. The carbide thickness depends ...

ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering

ZrB₂-based nanocomposites with and without carbon nanotubes (CNTs) as reinforcement were prepared at 1600 °C by spark plasma sintering. The effects of CNTs on the microstructure and mechanical properties of nano-ZrB₂ matrix composites were studied. The results indicated that adding CNTs can inhibit the abnormal grain growth of ZrB₂ grains and improve the fracture toughness of the composites. Th...

Fabrication of Nanostructured Cu matrix Nanocomposites by High Energy Mechanical Milling and Spark Plasma Sintering

Spark plasma sintering (SPS) is a sintering process that is capable of sintering hard worked powders in short times. This technique was used to fabricate bulk Cu and Cu-SiC nanocomposites. Pure Cu and mixed powders of Cu including 4 vol% of SiC nanoparticles were mechanically alloyed for 25 h and sintered at 750˚C under vacuum condition by SPS method. Microstructures of the materials were chara...

Zirconium Carbide Produced by Spark Plasma Sintering and Hot Pressing: Densification Kinetics, Grain Growth, and Thermal Properties

Spark plasma sintering (SPS) has been employed to consolidate a micron-sized zirconium carbide (ZrC) powder. ZrC pellets with a variety of relative densities are obtained under different processing parameters. The densification kinetics of ZrC powders subjected to conventional hot pressing and SPS are comparatively studied by applying similar heating and loading profiles. Due to the lack of ele...

Densification and preservation of ceramic nanocrystalline character by spark plasma sintering